Synthesis and structural properties of novel tricyclic 15-membered azalides
Summary: Starting from 3-decladinosyl-9a,11-cyclic carbamates of 15 membered azalide, strained tricyclic aglycone derivatives were prepared. The bridging 5-membered hemiketal ring was obtained by intramolecular ketalization of intermediary 3-keto derivative, whereas 5-membered ether derivatives were...
| Permalink: | http://skupni.nsk.hr/Record/nsk.NSK01000734970/Details |
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| Matična publikacija: |
Croatica chemica acta 82 (2009), 4 ; str. 715-723 |
| Glavni autor: | Fajdetić, Andrea, kemičarka (-) |
| Ostali autori: | Kobrehel, Gabrijela (-), Lazarevski, Gorjana, Marušić Ištuk, Zorica, Mutak, Stjepan |
| Vrsta građe: | Članak |
| Jezik: | eng |
| Predmet: | |
| Online pristup: |
Croatica Chemica Acta |
| LEADER | 01703caa a2200313 ir4500 | ||
|---|---|---|---|
| 001 | NSK01000734970 | ||
| 003 | HR-ZaNSK | ||
| 005 | 20170315093814.0 | ||
| 007 | ta | ||
| 008 | 100428s2009 ci ||| ||eng | ||
| 035 | |9 (HR-ZaNSK)737592 | ||
| 035 | |a (HR-ZaNSK)000734970 | ||
| 040 | |a HR-ZaNSK |b hrv |c HR-ZaNSK |e ppiak | ||
| 042 | |a croatica | ||
| 080 | |a 54 |2 MRF 1998. | ||
| 100 | 1 | |a Fajdetić, Andrea, |c kemičarka | |
| 245 | 1 | 0 | |a Synthesis and structural properties of novel tricyclic 15-membered azalides / |c Andrea Fajdetić, Gabrijela Kobrehel, Gorjana Lazarevski, Zorica Marušić-Ištuk, and Stjepan Mutak. |
| 300 | |b Ilustr. | ||
| 504 | |a Bibliografija: 27 jed | ||
| 520 | 8 | |a Summary: Starting from 3-decladinosyl-9a,11-cyclic carbamates of 15 membered azalide, strained tricyclic aglycone derivatives were prepared. The bridging 5-membered hemiketal ring was obtained by intramolecular ketalization of intermediary 3-keto derivative, whereas 5-membered ether derivatives were obtained by intramolecular Williamson-type displacement. In case of 12-O-alkyl derivatives complete diastereoslective formation of ethers was observed, while unsubstituted compound gave diastereomeric mixture. NMR analysis was used to confirm the structures of new tricyclic azalide compounds | |
| 653 | 0 | |a Triciklički azilidi |a Strukturna svojstva |a NMR analiza | |
| 700 | 1 | |a Kobrehel, Gabrijela | |
| 700 | 1 | |a Lazarevski, Gorjana | |
| 700 | 1 | |a Marušić Ištuk, Zorica | |
| 700 | 1 | |a Mutak, Stjepan | |
| 773 | 0 | |t Croatica chemica acta |x 0011-1643 |g 82 (2009), 4 ; str. 715-723 |w nsk.(HR-ZaNSK)000001621 | |
| 981 | |b B02/09 | ||
| 998 | |a Luko100428 |c vol2o130307 | ||
| 856 | 4 | 2 | |u http://hrcak.srce.hr/cca |y Croatica Chemica Acta |