GC-MS modified quechers method for multiresidue pesticide determination in red wine
This work reports a new selective and accurate multiresidue procedure for determination of 25 pesticides in red wine by GC-MS. Proposed procedure uses an original approach in sample preparation technique based on QuEChERS theory. Main focus of method development was modification of salts thus increa...
| Permalink: | http://skupni.nsk.hr/Record/nsk.NSK01001074277/Details |
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| Matična publikacija: |
Croatica chemica acta (Online) 92 (2019), 3 ; str. 419-428 |
| Glavni autori: | Pelajić, Maja (Author), Pelajić, Izidor, Mutavdžić Pavlović, Dragana, Vitali Čepo, Dubravka |
| Vrsta građe: | e-članak |
| Jezik: | eng |
| Predmet: | |
| Online pristup: |
https://doi.org/10.5562/cca3552 Hrčak |
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| 008 | 200916s2019 ci ad |o |0|| ||eng | ||
| 024 | 7 | |2 doi |a 10.5562/cca3552 | |
| 035 | |a (HR-ZaNSK)001074277 | ||
| 040 | |a HR-ZaNSK |b hrv |c HR-ZaNSK |e ppiak | ||
| 041 | 0 | |a eng |b eng | |
| 042 | |a croatica | ||
| 044 | |a ci |c hr | ||
| 080 | 1 | |a 54 |2 2011 | |
| 080 | 1 | |a 663 |2 2011 | |
| 100 | 1 | |a Pelajić, Maja |4 aut | |
| 245 | 1 | 0 | |a GC-MS modified quechers method for multiresidue pesticide determination in red wine |h [Elektronička građa] / |c Maja Pelajić, Izidor Pelajić, Dragana Mutavdžić Pavlović, Dubravka Vitali Čepo. |
| 246 | 3 | |a Gas chromatography-mass spectrometry | |
| 300 | |b Ilustr. ; graf. prikazi. | ||
| 504 | |a Bibliografija: 23 jed. | ||
| 504 | |a Abstract. | ||
| 520 | |a This work reports a new selective and accurate multiresidue procedure for determination of 25 pesticides in red wine by GC-MS. Proposed procedure uses an original approach in sample preparation technique based on QuEChERS theory. Main focus of method development was modification of salts thus increasing ionic strength of solution which improved pesticides partitioning and extraction efficiency. LOQs were in the range 0.01–250 μg L–1 with 56 % of target pesticides below or equal to 10 μg L–1. RSD for most pesticides was <20 % and recoveries were in the range 70–120 %. Matrix effect was found to be high for five pesticides confirming sample preparation procedure to be efficient. The proposed procedure was applied to 12 wine samples of different variety with determination of 40 % of target pesticides. Developed GC-MS methodology provides novel, selective and accurate approach for determination of 25 pesticide residues in red wine. | ||
| 653 | 0 | |a Vina |a Crno vino |a Pesticidi |a Plinska kromatografija |a Masena spektrometrija | |
| 700 | 1 | |a Pelajić, Izidor |4 aut | |
| 700 | 1 | |a Mutavdžić Pavlović, Dragana |4 aut | |
| 700 | 1 | |a Vitali Čepo, Dubravka |4 aut | |
| 773 | 0 | |t Croatica chemica acta (Online) |x 1334-417X |g 92 (2019), 3 ; str. 419-428 |w nsk.(HR-ZaNSK)000255036 | |
| 981 | |b Be2019 |b B05/19 | ||
| 998 | |b tino2010 | ||
| 856 | 4 | 0 | |u https://doi.org/10.5562/cca3552 |
| 856 | 4 | 0 | |u https://hrcak.srce.hr/227021 |y Hrčak |
| 856 | 4 | 1 | |y Digitalna.nsk.hr |